Structure

    redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6b1D-GlcNAc,p--??1D-Gal,p$MONO,Und,-H,0,redEnd

Effects of size and geographical origin on Atlantic salmon, Salmo salar, mucin O-glycan repertoire

PubMed Entry

GlyTouCan Accession Number: Loading...

Peak Intensity
317.19 1.3
328.8 1.2
347.04 1.9
364.07 8.9

Annotations:

BY ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd CZ ?1D-GalNAc,p/#ccleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd B a1D-GalNAc,p/#bcleavage--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
364.4 1.0
365.46 2.1
377.09 1.3
381.46 2.0
381.97 4.4

Annotations:

CY ?1D-GalNAc,p/#ccleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd C a1D-GalNAc,p/#ccleavage--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
382.27 1.4
386.52 1.2
387.3 2.0
388.94 1.2

Annotations:

ZZ redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd
406.24 1.1
406.92 1.6

Annotations:

YZ redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
419.23 0.9
424.11 1096.7

Annotations:

^{0,4}A_{GalNAc} a1D-GalNAc,p/#acleavage_0_4--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
425.12 101.1

Annotations:

YY redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
438.4 1.5
447.52 2.8
466.46 1.6
467.45 1.9
474.31 1.1
507.05 1.3
508.94 0.9
521.32 1.1
526.54 0.9
527.5 1.3
531.22 8.1
532.38 1.9
532.8 0.8
545.07 0.8
549.19 26.7

Annotations:

BZ ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd BZ ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
549.89 1.4
550.4 2.5
567.12 21.3

Annotations:

BY ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd BY ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd CZ ?1D-GalNAc,p/#ccleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd CZ ?1D-GalNAc,p/#ccleavage--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
567.33 9.9
567.78 3.6
568.27 3.4
568.53 2.3
569.12 14.5

Annotations:

Z redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd
569.5 1.9
570.26 2.1
583.12 0.9
586.08 1.8
587.18 2.1

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
588.16 1.6
627.3 1.1
640.11 1.7
652.12 1.1
670.11 4.6
675.14 1.3
681.82 1.2
688.34 3.2
695.29 0.9
712.21 58.9
713.27 17.5
729.28 28.2

Annotations:

B ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
730.22 68.2

Annotations:

^{2,4}X_{HexNAc} redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#xcleavage_2_4$MONO,Und,-H,0,redEnd
731.25 8.8
731.52 3.7
748.36 2.8
754.27 3.7
755.25 0.8
757.87 0.8
772.37 23.3

Annotations:

Z redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
773.34 5.6
790.35 9.4

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
790.94 3.3
791.32 1.9
791.61 1.9
792.31 1.2
802.06 5.7
802.45 5.3
803.26 3.9
812.44 1.2
820.17 1.8
832.29 7.6
833.28 1.9
842.99 1.7
844.28 44.6
845.16 2.3
849.9 1.2
850.19 12.6
851.25 2.0
855.96 1.2
856.39 2.0
862.12 2.1
862.41 5.0
863.31 1.6
873.94 1.8
874.31 5.5
874.6 1.6
892.27 714.7
893.3 189.9
909.66 2.3
910.26 74.2
911.37 20.3
916.43 2.3
922.42 0.8

There are 4 similar spectra:

Id Structure Score

1.00

5734

1.00

7412

0.97

7441

0.97

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 951.37
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Salmo Salar
Tissue - Mucus

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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