Structure

    redEnd--??1D-GalNAc,p--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd

The O-glycome of human nigrostriatal tissue and its alteration in Parkinsons disease

GlyTouCan Accession Number: Loading...

Peak Intensity
138.93 3.3

Annotations:

^{0,4}A_{Gal} b1D-Gal,p/#acleavage_0_4--6?1S$MONO,Und,-H,0,redEnd
142.68 0.8
143.26 1.5
150.74 1.7
152.98 2.6

Annotations:

^{3,5}A_{Gal} b1D-Gal,p/#acleavage_3_5--6?1S$MONO,Und,-H,0,redEnd
156.15 2.1
162.92 0.8
168.94 2.8

Annotations:

^{0,3}A_{Gal} b1D-Gal,p/#acleavage_0_3--6?1S$MONO,Und,-H,0,redEnd
171.05 1.2
177.02 0.8
177.29 0.8
179.07 0.8

Annotations:

C ?1D-GalNAc,p/#ccleavage--3b1D-Gal,p--6?1S/#lcleavage$MONO,Und,-H,0,redEnd
180.89 3.8
181.11 4.9
198.76 6.4

Annotations:

^{0,2}A_{Gal} b1D-Gal,p/#acleavage_0_2--6?1S$MONO,Und,-H,0,redEnd
199.05 5.6

Annotations:

^{0,2}A_{Gal} b1D-Gal,p/#acleavage_0_2--6?1S$MONO,Und,-H,0,redEnd
203.97 4.0

Annotations:

Z redEnd--??1D-GalNAc,p--3b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
204.25 1.3

Annotations:

Z redEnd--??1D-GalNAc,p--3b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
204.94 1.7
205.17 0.8
207.04 1.0
209.1 0.8
222.05 1.2

Annotations:

Y redEnd--??1D-GalNAc,p--3b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
222.25 0.9

Annotations:

Y redEnd--??1D-GalNAc,p--3b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
223.06 7.8
224.98 0.9
227.44 0.8
239.89 0.8
241.04 276.9

Annotations:

B ?1D-GalNAc,p/#bcleavage--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
241.88 9.9
242.11 10.3
243.04 4.6
249.91 0.8
253.23 1.1
257.01 1.8
259.05 17.0

Annotations:

C ?1D-GalNAc,p/#ccleavage--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
260.07 1.3
261.14 5.6
262.33 0.8

Annotations:

^{1,3}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_3--3b1D-Gal,p--6?1S/#lcleavage$MONO,Und,-H,0,redEnd
265.23 1.3

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5--3b1D-Gal,p--6?1S/#lcleavage$MONO,Und,-H,0,redEnd
268.88 1.1
269.19 1.0
284.13 7.3
285.13 0.8
288.93 0.9
299.06 1.0
301.26 0.8

Annotations:

^{2,4}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_4--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
302.2 22.5
303.08 2.3
303.32 1.0
313.23 0.9
315.16 0.9
316.05 0.9
319.31 1.3
320.88 1.2
327.16 1.5
344.23 0.8
344.74 0.9

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
345.1 3.5

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
345.86 2.1
350.21 0.8
356.41 1.7
357.16 0.8
359.08 0.8
361.2 3.8

Annotations:

^{0,2}A_{GalNAc} ?1D-GalNAc,p/#acleavage_0_2--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
364.18 2.7
365.07 2.6
366.02 15.6
367.04 1.0
370.22 1.1
374.15 2.5
375.92 1.7
377.03 1.9
377.4 0.9
383.43 1.5
384.18 3.7

Annotations:

redEnd--??1D-GalNAc,p--3b1D-Gal,p--6?1S/#lcleavage$MONO,Und,-H,0,redEnd
385.26 2.4
391.8 0.9
392.14 1.0
402.01 3.6
402.26 1.4
403.18 1.1
404.2 15.4
405.13 15.3
410.15 2.7
416.14 1.0

Annotations:

^{1,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_5--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
416.34 1.1

Annotations:

^{1,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_5--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
417.07 1.6
418.44 2.2
419.81 0.9
420.18 7.8
421.16 2.8
422.29 8.5
426.52 0.9
428.22 4.6
429.08 1.1
433.63 0.8
434.25 1.8
464.17 35.7

Annotations:

redEnd--??1D-GalNAc,p--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
465.3 4.2

There are 1 similar spectra:

Id Structure Score

1.00

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 463.12
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Homo Sapiens
Tissue - Brain

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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