Structure

    redEnd--??1D-Man,p--2b1D-GlcNAc,p--??1D-Gal,p$MONO,Und,-H,0,redEnd

The O-glycome of human nigrostriatal tissue and its alteration in Parkinsons disease

GlyTouCan Accession Number: Loading...

Peak Intensity
160.99 18.7

Annotations:

B b1D-GlcNAc,p/#bcleavage--??1D-Gal,p$MONO,Und,-H,0,redEnd
162.99 3.9

Annotations:

Z redEnd--??1D-Man,p--2b1D-GlcNAc,p/#zcleavage$MONO,Und,-H,0,redEnd
166.18 1.1
172.35 1.1
178.31 1.1
178.99 282.8

Annotations:

C b1D-GlcNAc,p/#ccleavage--??1D-Gal,p$MONO,Und,-H,0,redEnd
180.04 1.6
181.08 16.9

Annotations:

Y redEnd--??1D-Man,p--2b1D-GlcNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
184.07 4.9

Annotations:

BZ ?1D-Man,p/#bcleavage--2b1D-GlcNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
201.08 1.4
202.05 47.5

Annotations:

BY ?1D-Man,p/#bcleavage--2b1D-GlcNAc,p--??1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd CZ ?1D-Man,p/#ccleavage--2b1D-GlcNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
208.13 1.5
208.91 1.7
219.92 1.5

Annotations:

CY ?1D-Man,p/#ccleavage--2b1D-GlcNAc,p--??1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
221.12 6.8
238.1 1.0
241.19 1.0
241.86 0.9
243.86 1.7

Annotations:

^{1,3}A_{Man}Z ?1D-Man,p/#acleavage_1_3--2b1D-GlcNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
255.96 2.0
256.66 1.4
258.07 1.0
259.37 1.3
262.94 31.4
263.42 2.9
270.54 1.2
281.12 4.4
301.28 1.3
302.03 1.0
304.15 1.3
306.17 1.3
311.32 0.9
315.22 0.9
317.21 2.1
317.9 1.1

Annotations:

^{1,5}A_{Man}Z ?1D-Man,p/#acleavage_1_5--2b1D-GlcNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
318.23 1.7

Annotations:

^{1,5}A_{Man}Z ?1D-Man,p/#acleavage_1_5--2b1D-GlcNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
319.2 2.8
323.87 4.0
324.17 7.1
327.29 1.0
330.94 1.3
331.28 1.3
337.28 5.1
341.19 1.0
343.12 1.6
346.16 1.4
363.24 1.7
364.2 96.9

Annotations:

B ?1D-Man,p/#bcleavage--2b1D-GlcNAc,p--??1D-Gal,p$MONO,Und,-H,0,redEnd
365.32 1.0
366.17 64.6

Annotations:

Z redEnd--??1D-Man,p--2b1D-GlcNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
374.48 1.0
384.25 6.0

Annotations:

Y redEnd--??1D-Man,p--2b1D-GlcNAc,p--??1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
385.93 1.2
386.24 1.5
387.04 1.1
392.06 1.2
396.25 4.2
401.05 1.6
408.07 0.9
412.22 1.4
413.42 1.3
414.37 2.7
425.18 1.5
427.45 0.9
430.11 2.4
431.31 1.1
437.31 1.1
446.27 2.5
447.03 1.1
448.3 6.1
449.1 1.5
449.49 1.0
454.18 1.2

Annotations:

^{1,4}A_{Man} ?1D-Man,p/#acleavage_1_4--2b1D-GlcNAc,p--??1D-Gal,p$MONO,Und,-H,0,redEnd
455.07 2.2
456.13 1.4
459.07 4.8
464.1 1.5
464.37 1.4
466.19 3.9
466.88 1.1
471.17 1.2
474.01 1.2
477.25 1.1
482.56 3.5
483.42 1.8
484.27 3.4
484.49 1.0
486.29 63.9
487.1 1.7
487.38 1.4
492.24 1.0
502.27 8.7
504.25 95.6
505.99 1.0
506.62 1.1
509.65 2.8
510.33 8.4
510.94 2.2
512.37 1.7
514.2 1.3

There are 2 similar spectra:

Id Structure Score

1.00

5544

0.92

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 545.21
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Homo Sapiens
Tissue - Brain

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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