MIRAGE upload

redEnd--??2D-NeuAc,p--?a2D-NeuAc,p$MONO,Und,-H,0,redEnd

The O-glycome of human nigrostriatal tissue and its alteration in Parkinsons disease

GlyTouCan Accession Number: Loading...

Peak	Intensity
169.54	2.4
170.15	3.3
183.07	1.5
184.09	0.9
190.15	1.2
199.9	1.4
202.08	21.5
202.41	2.5
229.15	3.7
232.1	52.5
246.89	1.5
250.13	8.7
256.31	1.9
262.13	1.1
265.04	1.6
271.02	2.1
274.21	3.3
274.97	2.6
276.51	1.3
277.0	1.7
281.25	0.4
285.12	7.1
290.18	28.3
Annotations: B
291.08	6.7
292.14	43.8
Annotations: Z
294.04	2.2
309.13	0.6
310.18	141.9
Annotations: Y
310.97	0.5
311.32	7.5
311.87	0.0
316.05	0.5
317.29	0.5
325.04	5.7
329.28	1.1
335.17	2.4
336.23	2.3
337.18	1.2
339.09	1.9
341.11	1.2
344.15	1.6
347.12	2.2
352.4	1.1
354.06	1.9
363.46	2.8
365.19	1.4
367.15	1.3
373.23	1.1
374.08	2.6
381.09	3.3
381.42	1.2
382.05	0.7
387.03	1.0
400.97	0.6
406.09	1.9
410.23	1.2
Annotations: ^{0,4}A_{NeuAc}
416.17	4.8
420.27	2.0
429.33	1.3
437.11	5.8
439.26	2.4
445.27	7.6
446.82	2.9
448.05	1.1
449.23	4.4
456.42	1.2
463.25	1.2
467.9	0.7
475.33	5.5
477.21	1.7
479.23	20.0
484.45	1.7
487.12	1.3
497.09	1.1
503.06	5.4
503.33	1.1
505.24	4.5
505.64	3.4
513.37	5.5
514.15	1.7
517.47	1.5
518.79	0.5
520.75	2.1
521.34	9.4
533.45	4.7
537.36	1.0
538.21	0.8
538.58	0.7
539.3	3.8
541.16	0.6
547.36	0.6
556.99	2.7
557.36	2.0
560.27	0.6
564.83	5.3
565.43	36.6
566.19	9.8
570.57	0.5
571.36	0.9
626.28	0.8

There are not related spectra

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 600.22
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Homo Sapiens

HPLC

Column

Method

78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
10 mM (NH4)HCO3
10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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