Structure

    redEnd--??1D-Man,p--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p)--??1S$MONO,Und,-H,0,redEnd

The O-glycome of human nigrostriatal tissue and its alteration in Parkinsons disease

GlyTouCan Accession Number: Loading...

Peak Intensity
255.02 33.0
256.15 1.4
271.0 1.8
290.16 2.4
299.98 1.2
314.38 1.4
352.26 2.9
379.47 2.5
397.22 1.5
400.35 1.2
405.18 1.5
444.33 5.8

Annotations:

BY ?1D-Man,p/#bcleavage--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p/#ycleavage)--??1S$MONO,Und,-H,0,redEnd CZ ?1D-Man,p/#ccleavage--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p/#zcleavage)--??1S$MONO,Und,-H,0,redEnd
452.49 2.2
471.29 1.5
472.21 3.2
477.41 1.7
485.29 1.8
490.33 1.6
497.22 1.6
497.43 1.5
515.31 7.2
516.02 1.2
521.86 1.8
529.41 7.0
529.8 1.3
530.15 1.4
539.01 1.3
541.25 2.1
541.59 2.9
546.41 2.2

Annotations:

Y redEnd--??1D-Man,p--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p/#ycleavage)--??1S/#lcleavage$MONO,Und,-H,0,redEnd
553.53 3.5
559.29 6.7
559.78 2.1
572.13 3.4
573.07 2.1
574.07 1.5
580.5 1.9
582.13 1.9
584.39 1.7
587.57 1.8
602.36 1.5
604.32 1.6
608.31 2.6

Annotations:

Z redEnd--??1D-Man,p--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p/#zcleavage)--??1S$MONO,Und,-H,0,redEnd
618.71 1.5
620.21 3.2

Annotations:

B ?1D-Man,p/#bcleavage--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p)--??1S$MONO,Und,-H,0,redEnd
622.33 1.6
623.87 1.3
626.11 35.6

Annotations:

Y redEnd--??1D-Man,p--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p/#ycleavage)--??1S$MONO,Und,-H,0,redEnd
626.38 32.7

Annotations:

Y redEnd--??1D-Man,p--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p/#ycleavage)--??1S$MONO,Und,-H,0,redEnd
627.26 13.0
631.28 1.5
635.59 2.2
639.75 1.5
640.22 1.7
648.33 1.3
650.27 1.3
654.21 1.7
669.53 1.9
670.17 1.4
684.06 1.7
685.19 2.1
694.54 1.3
701.84 5.1
703.37 2.4
704.33 5.8
709.43 2.0
711.81 1.4
714.27 1.4
715.05 1.6
720.24 4.4
721.39 6.2
722.34 517.8

Annotations:

redEnd--??1D-Man,p--??1D-GlcNAc,p--??1D-Gal,p(--??1HexA,p)--??1S/#lcleavage$MONO,Und,-H,0,redEnd
723.37 76.4
726.05 2.0
727.34 6.8
727.62 5.1
728.5 4.6
730.02 1.5
730.41 5.4
735.5 3.5
738.52 4.7
739.28 13.7
740.36 8.6
741.19 3.8
741.49 4.3
742.53 1.8
743.42 1.6
749.78 2.7
753.28 4.5
753.57 3.7
754.52 4.4
756.6 1.7
757.4 10.9
758.43 4.9
759.36 1.9
765.55 2.1
766.34 4.0
770.48 2.7
771.42 48.3
772.53 9.8

There are 1 similar spectra:

Id Structure Score

1.00

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 801.20
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Homo Sapiens
Tissue - Brain

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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