Structure

    redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd

The O-glycome of human nigrostriatal tissue and its alteration in Parkinsons disease

GlyTouCan Accession Number: Loading...

Peak Intensity
452.28 0.3

Annotations:

B ?1D-GalNAc,p/#bcleavage--3b1D-Gal,p--3a2D-NeuAc,p$MONO,Und,-H,0,redEnd B b1D-GlcNAc,p/#bcleavage--4b1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
452.85 0.0
569.28 1.1

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
569.95 0.0
575.25 0.4
575.8 0.0
581.23 0.6
581.79 0.0
587.18 1.9

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
587.54 0.6

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
588.11 0.0
647.38 0.4
647.94 0.0
689.49 0.6
690.04 0.0
714.17 0.3
714.7 0.0
724.48 0.8
725.03 0.0
745.23 2.8

Annotations:

^{0,3}A_{GalNAc} ?1D-GalNAc,p/#acleavage_0_3--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
745.78 0.0
746.3 0.0
748.94 0.8

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
749.44 20.7

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
750.2 0.0
763.03 1.1
763.61 0.0
799.2 1.7
799.77 0.0
819.34 0.7
819.88 0.0
842.5 0.6
843.06 0.0
856.65 1.8
857.2 0.0
860.25 1.2

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
860.79 0.0

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
879.38 0.5
879.94 0.0
930.18 0.7
930.71 0.0
948.56 0.7
949.12 0.0
962.43 1.4
963.01 0.0
996.07 1.8
996.33 0.5
996.88 0.0
1021.23 1.3
1021.78 0.0
1022.54 7.2

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
1023.13 0.0
1023.68 0.0
1038.35 4.3
1038.71 0.9
1039.64 10.5
1040.44 318.2

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
1041.56 9.2
1042.15 0.0
1042.55 1.0
1043.11 0.0
1069.28 1.3
1069.83 0.0
1072.55 0.6
1073.11 0.0
1117.05 2.4
1117.61 0.0
1126.44 0.6
1127.02 0.0
1151.66 0.9
1152.2 0.0
1185.64 2.4
1186.2 0.0
1191.45 1.8
1192.02 0.0
1193.58 1.1
1194.12 0.0
1195.96 1.6
1196.52 0.0
1201.52 0.5
1202.08 0.0
1206.91 0.8
1207.45 0.0
1232.46 0.3
1233.02 0.0
1253.25 0.8
1253.6 0.5
1254.14 0.0
1271.52 0.3
1272.08 0.0
1277.12 1.0
1277.38 0.6
1277.95 0.0
1286.35 0.5
1287.22 0.6
1287.62 8.2
1288.26 0.0
1295.58 0.3
1295.75 0.5
1296.29 0.0

There are 23 similar spectra:

Id Structure Score

1.00

3522

1.00

5849

1.00

5474

1.00

4255

1.00

5247

1.00

4913

1.00

1.00

5530

1.00

7637

1.00

3788

1.00

7226

1.00

5217

1.00

4087

1.00

5531

0.99

7660

0.99

7676

0.99

0.99

7415

0.99

7444

0.99

3992

0.95

0.94

3993

0.85

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 1330.48
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Homo Sapiens
Tissue - Brain

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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