Structure

    redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd

The intestinal O-glycome is modified by reactive oxygen species deficiency

GlyTouCan Accession Number: Loading...

Peak Intensity
263.98 2.6
282.05 119.1

Annotations:

B ?1D-GalNAc,p/#bcleavage--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
283.05 7.9
302.01 1.6
342.14 3.4
343.08 1.5
358.27 1.3
371.89 2.4
372.15 5.3
385.89 1.7
386.28 3.1
387.08 7.0
387.32 2.0
407.31 10.6

Annotations:

Z redEnd--??1D-GalNAc,p(--??1D-Gal,p/#zcleavage)--??1D-GlcNAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
408.3 1.4
410.33 1.6
415.28 1.7
425.27 2.5

Annotations:

Y redEnd--??1D-GalNAc,p(--??1D-Gal,p/#ycleavage)--??1D-GlcNAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
427.31 13.8
428.22 3.9
444.34 2.0
445.22 12.3
446.15 3.5
450.87 1.6
451.12 2.2
457.17 1.5
463.25 2.0
464.36 3.5
469.27 3.1
486.26 5.6
487.28 65.2

Annotations:

Z redEnd--??1D-GalNAc,p(--??1D-Gal,p/#zcleavage)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
488.23 7.1
488.51 2.8
505.26 1267.7

Annotations:

Y redEnd--??1D-GalNAc,p(--??1D-Gal,p/#ycleavage)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
506.26 231.0
507.25 5.4
508.34 1.3
532.52 1.5
548.28 2.5
569.09 1.3

Annotations:

Z redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p/#zcleavage)--??1D-GlcNAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
577.43 3.6
587.17 1.5

Annotations:

Y redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p/#ycleavage)--??1D-GlcNAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
591.21 1.4
596.06 1.5
607.18 10.9
607.46 7.6
609.33 2.1
610.26 3.3
611.08 1.2
620.81 1.8
625.45 5.1
626.48 1.6
637.32 2.9
649.1 11.1

Annotations:

Z redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p/#zcleavage)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
649.39 12.3

Annotations:

Z redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p/#zcleavage)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
650.16 3.7
651.04 1.5
651.37 3.1
652.46 1.3
659.25 2.6
665.53 2.3
666.37 5.4
667.3 2857.1

Annotations:

Y redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p/#ycleavage)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
668.28 738.7
669.24 6.6
669.77 1.2
670.35 3.2
687.37 1.4
693.51 2.8
694.26 8.1
709.45 5.2
711.39 2.7
715.04 3.4
718.1 2.1
720.52 1.4
722.35 1.4
722.72 2.7
731.45 2.4
733.52 2.8

Annotations:

redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
738.12 1.3
739.35 2.9
739.59 1.9
750.49 1.4
751.24 1.2
752.78 1.6
753.39 18.9
754.39 9.0
759.53 1.2
763.74 2.9
769.33 1.4
771.27 9.6
772.54 1.6
778.4 2.0
782.39 5.3
783.32 3.1
794.55 2.5
795.48 1.8
795.77 1.3
813.25 1.6

Annotations:

redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
813.57 2.7

Annotations:

redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd

There are 8 similar spectra:

Id Structure Score

7651

1.00

6726

1.00

5781

1.00

3121

1.00

5566

0.98

5780

0.95

4263

0.83

6725

0.82

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 812.25
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

N/A

MIRAGE Structural data

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