test

test, Manuscript

Retention Time Recorded Precursor Mass Structure
13.08 384.23 [M -1H]1- redEnd--??1D-GalNAc,p--3b1D-Gal,p$MONO,Und,-H,0,redEnd
17.46 667.42 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
17.91 675.42 [M -1H]1- redEnd--??1D-GalNAc,p--??1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
18.6 749.3 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p)--??1D-GlcNAc,p--??1D-Gal,p$MONO,Und,-H,0,redEnd
19.21 975.53 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p)--??1D-GlcNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1S$MONO,Und,-H,0,redEnd
19.77 895.3 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p)--??1D-GlcNAc,p--3b1D-Gal,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
21.58 1331.56 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??2D-NeuAc,p)--??1D-GlcNAc,p(--??1D-Gal,p)--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
22.35 895.3 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p)--??1D-GlcNAc,p--??1D-Gal,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
26.57 530.2 [M -1H]1- redEnd--??1D-GalNAc,p--??1D-Gal,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
27.02 895.3 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1D-Gal,p$MONO,Und,-H,0,redEnd
27.2 1041.55 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1D-Gal,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
28.3 1121.61 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1S$MONO,Und,-H,0,redEnd
28.34 813.24 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1S$MONO,Und,-H,0,redEnd
28.55 1041.55 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1D-Gal,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
28.6 1186.65 [M -1H]1- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p--??1D-Gal,p--??2D-NeuAc,p$MONO,Und,-H,0,redEnd
29.3 738.26 [M -2H]2- redEnd--??1D-GalNAc,p(--??1D-Gal,p--??1L-Fuc,p)--??1D-GlcNAc,p(--??1D-Gal,p--??2D-NeuAc,p)--??2D-NeuAc,p$MONO,Und,-2H,0,redEnd

Structure Format

SNFG Oxford Text

Biological Context

N/A

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

N/A

MIRAGE

See report

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