Structure

    redEnd--??1D-GalNAc,p(--3b1D-Gal,p)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p$MONO,Und,-H,0,redEnd

Rainbow trout gastrointestinal mucus, mucin production, mucin glycosylation and response to lipopolysaccharide

GlyTouCan Accession Number: Loading...

Peak Intensity
329.41 1.4
347.1 1.5
347.44 3.0
364.19 12.2

Annotations:

BY ?1D-GalNAc,p/#bcleavage--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd CZ ?1D-GalNAc,p/#ccleavage--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd
365.35 1.7
371.16 1.5
389.12 27.4

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
389.38 25.6
390.09 3.0
390.45 2.4
406.12 1.5
407.3 8.7

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
412.34 2.1
424.28 2.8
449.4 1.7
462.29 2.6
474.34 2.3
509.11 3.6
509.41 5.5
512.51 4.3
527.39 19.2

Annotations:

^{2,4}X_{GlcNAc} redEnd--??1D-GalNAc,p(--3b1D-Gal,p)--6b1D-GlcNAc,p/#xcleavage_2_4$MONO,Und,-H,0,redEnd
527.76 2.4
528.21 2.1

Annotations:

C ?1D-GalNAc,p/#ccleavage--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p$MONO,Und,-H,0,redEnd
530.28 1.5
541.12 1.6
551.54 1.9

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd
552.43 7.3
567.61 1.5
569.31 294.3

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd
570.39 31.9

Annotations:

^{0,4}A_{GalNAc} ?1D-GalNAc,p/#acleavage_0_4--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p$MONO,Und,-H,0,redEnd
587.27 2.8

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd
596.23 2.0
610.08 2.9
612.29 1.5
618.71 2.3
622.35 1.5
651.23 1.4
655.29 7.8
658.41 1.7
670.36 1.6
671.32 1.8
673.42 4.9
678.81 1.5
680.37 3.1
682.18 1.6
686.06 1.7
686.4 1.7
715.49 17.0

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p$MONO,Und,-H,0,redEnd
716.51 5.3
718.56 1.7
722.37 1.5
723.43 1.5
726.28 1.6
731.5 4.4

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd
733.31 7.3

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p$MONO,Und,-H,0,redEnd
733.67 3.8
734.4 2.4
746.52 1.8
749.44 3.4

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p)--6b1D-GlcNAc,p--4b1D-Gal,p--2a1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd
768.64 1.6
772.68 1.5
773.49 1.5
774.11 2.0
775.56 2.8
783.43 1.6
789.09 2.2
790.27 1.8
791.69 1.8
796.54 3.5
803.26 1.6
804.41 2.3
805.47 1.8
808.81 1.7
814.32 2.1
815.61 1.7
826.66 1.4
833.61 1.8
835.33 20.1
835.59 10.1
836.44 4.7
837.97 1.6
847.31 2.5
851.42 4.5
851.73 3.6
852.21 5.6
852.49 3.9
852.74 1.5
853.49 39.5
854.2 2.3
854.74 9.7
858.69 2.9
859.32 3.2
859.71 5.5
860.52 1.7
864.49 1.7
865.45 2.9
866.72 2.0

There are 10 similar spectra:

Id Structure Score

5792

0.99

3885

0.98

7654

0.98

7670

0.98

5579

0.98

7225

0.97

4244

0.97

5236

0.97

3127

0.97

5789

0.80

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 894.35
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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