Structure

    redEnd--??1D-GalNAc,p--3b1D-Gal,p$MONO,Und,-H,0,redEnd

Rainbow trout mucus O-glycosylation

GlyTouCan Accession Number: Loading...

Peak Intensity
250.21 0.2
250.77 0.0
251.3 0.0
255.73 0.0
256.28 0.0
256.84 0.0
262.86 0.6

Annotations:

^{1,3}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_3--3b1D-Gal,p$MONO,Und,-H,0,redEnd
263.78 0.2
263.99 0.1
264.52 0.0

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5--3b1D-Gal,p$MONO,Und,-H,0,redEnd
264.93 0.2

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5--3b1D-Gal,p$MONO,Und,-H,0,redEnd
265.52 0.0

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5--3b1D-Gal,p$MONO,Und,-H,0,redEnd
266.03 0.0

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5--3b1D-Gal,p$MONO,Und,-H,0,redEnd
267.0 0.1
267.54 0.0
268.1 0.0
269.13 0.2
269.69 0.0
270.24 0.0
273.39 0.1
273.95 0.0
274.5 0.0
276.12 5.8
277.1 0.4
277.46 0.0
277.67 0.0
278.19 0.0
284.6 0.3
285.19 0.0
285.46 0.3
286.02 0.0
286.54 0.0
291.3 0.2

Annotations:

^{1,4}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_4--3b1D-Gal,p$MONO,Und,-H,0,redEnd
291.86 0.0

Annotations:

^{1,4}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_4--3b1D-Gal,p$MONO,Und,-H,0,redEnd
292.38 0.0

Annotations:

^{1,4}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_4--3b1D-Gal,p$MONO,Und,-H,0,redEnd
293.25 0.1
293.79 0.0
294.35 0.0
308.86 0.1
309.44 0.0
309.95 0.0
312.8 0.3
313.14 0.1
313.7 0.0
314.23 0.0
316.87 0.1
317.44 0.0
317.96 0.0
319.25 0.2
319.65 0.1
320.2 0.0
320.77 0.0
321.41 0.1
321.96 0.0
322.52 0.0
323.2 0.2
324.23 5.0
324.84 0.0
325.43 0.7
325.98 0.0
326.54 0.0
328.31 0.2
329.09 0.1
329.4 0.2
329.95 0.0
330.52 0.0
332.84 0.2
333.38 0.0
333.94 0.0
334.21 0.1
334.77 0.0
335.28 0.0

Annotations:

^{1,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_5--3b1D-Gal,p$MONO,Und,-H,0,redEnd
340.2 0.1
340.5 0.1
341.04 0.0
341.61 0.0
341.98 0.2
342.27 0.9
342.84 0.0
343.4 0.0
347.74 0.1
348.3 0.0
348.86 0.0
349.32 0.1
349.87 0.0
350.41 0.0
352.97 0.3
353.53 0.0
353.88 0.1
354.44 0.0
354.96 0.0
356.03 0.1
356.6 0.0
357.12 0.0
358.25 0.2
358.8 0.0
359.36 0.0
385.4 0.1
385.95 0.0
386.51 0.0

There are 1 similar spectra:

Id Structure Score

7132

0.78

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 383.16
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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