Ion Mobility-Tandem Mass Spectrometry of Mucin-type O-Glycans: from Cystic Fibrosis Sputum
The MS/MS data was generated after TIMS separation and retention time refers to CCS values in Ų
GlyTouCan Accession Number:
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| Peak | Intensity |
|---|---|
| 100.8948 | 1.2 |
|
Annotations: ^{2,4}A_{GalNAc}Z |
|
| 103.7745 | 1.1 |
| 108.5976 | 1.0 |
| 113.5185 | 1.2 |
| 118.3537 | 1.0 |
| 124.6535 | 1.1 |
| 155.1887 | 1.3 |
| 180.2692 | 1.3 |
| 180.5729 | 1.1 |
| 187.4359 | 1.3 |
| 192.0039 | 1.3 |
| 206.0923 | 1.1 |
| 215.741 | 1.3 |
| 232.2703 | 1.3 |
| 236.5113 | 1.2 |
| 265.2634 | 1.1 |
|
Annotations: C^{2,5}X_{NeuAc} |
|
| 270.1065 | 1.3 |
| 272.0871 | 1.2 |
| 272.7169 | 2.0 |
| 290.0776 | 31.2 |
|
Annotations: B |
|
| 290.0859 | 37.4 |
|
Annotations: B |
|
| 290.0961 | 37.5 |
|
Annotations: B |
|
| 290.1276 | 1.7 |
|
Annotations: B |
|
| 290.1886 | 2.1 |
|
Annotations: B |
|
| 291.0889 | 9.0 |
|
Annotations: ^{1,4}A_{GalNAc} |
|
| 291.1162 | 1.5 |
|
Annotations: ^{1,4}A_{GalNAc} |
|
| 292.1138 | 2.3 |
|
Annotations: ^{1,4}A_{GalNAc}Y |
|
| 292.1218 | 1.4 |
|
Annotations: ^{1,4}A_{GalNAc}Y |
|
| 305.1143 | 1.4 |
| 346.0977 | 1.8 |
| 384.146 | 6.9 |
|
Annotations: YY |
|
| 403.1825 | 1.1 |
| 408.1656 | 1.5 |
|
Annotations: B^{1,3}X_{NeuAc} |
|
| 451.1877 | 1.8 |
|
Annotations: ^{0,2}A_{GalNAc}Z |
|
| 451.1994 | 1.9 |
|
Annotations: ^{0,2}A_{GalNAc}Z |
|
| 452.1895 | 1.1 |
|
Annotations: B |
|
| 454.1554 | 1.1 |
|
Annotations: Y^{1,4}X_{NeuAc} |
|
| 469.1667 | 1.0 |
| 470.1513 | 2.7 |
|
Annotations: C |
|
| 471.163 | 1.0 |
| 495.1773 | 1.3 |
| 510.1911 | 2.1 |
|
Annotations: CZ |
|
| 514.1922 | 1.1 |
| 521.1979 | 10.7 |
| 522.1955 | 1.6 |
| 522.2266 | 1.0 |
| 524.8209 | 1.0 |
|
Annotations: Z^{1,5}X_{Fuc} |
|
| 535.2187 | 1.0 |
|
Annotations: ^{1,4}X_{NeuAc}Y |
|
| 544.7102 | 1.1 |
| 551.2081 | 2.6 |
| 552.2029 | 1.5 |
|
Annotations: ^{0,4}A_{GalNAc}Z |
|
| 553.221 | 1.5 |
|
Annotations: ^{1,3}A_{GalNAc} |
|
| 553.237 | 2.1 |
|
Annotations: ^{1,3}A_{GalNAc} |
|
| 554.2333 | 1.2 |
| 568.2028 | 1.1 |
| 569.2203 | 4.0 |
| 569.2515 | 1.0 |
| 570.1911 | 2.4 |
|
Annotations: ^{0,4}A_{GalNAc}Y |
|
| 570.2166 | 1.7 |
|
Annotations: ^{0,4}A_{GalNAc}Y |
|
| 571.2371 | 2.8 |
|
Annotations: YY |
|
| 575.217 | 1.4 |
| 592.7227 | 1.4 |
|
Annotations: Y |
|
| 593.2122 | 1.3 |
| 627.7186 | 1.1 |
|
Annotations: ^{0,2}X_{NeuAc} |
|
| 631.2467 | 2.8 |
|
Annotations: ^{1,3}X_{NeuAc}Y |
|
| 631.2676 | 5.6 |
|
Annotations: ^{1,3}X_{NeuAc}Y |
|
| 639.2045 | 1.1 |
| 655.2012 | 1.3 |
|
Annotations: BY |
|
| 655.2176 | 2.5 |
|
Annotations: BY |
|
| 657.2161 | 3.8 |
|
Annotations: Z |
|
| 657.2372 | 6.9 |
|
Annotations: Z |
|
| 658.2399 | 1.9 |
| 673.2696 | 1.2 |
|
Annotations: CY |
|
| 675.2465 | 19.0 |
|
Annotations: Y |
|
| 675.2968 | 1.6 |
|
Annotations: Y |
|
| 676.2472 | 4.8 |
| 677.2402 | 1.7 |
| 677.2691 | 1.3 |
| 704.3759 | 1.0 |
|
Annotations: C^{1,4}X_{NeuAc} |
|
| 707.7518 | 1.0 |
| 710.266 | 1.5 |
| 715.2551 | 2.7 |
|
Annotations: ^{0,4}A_{GalNAc}Y |
|
| 715.2771 | 3.8 |
|
Annotations: ^{0,4}A_{GalNAc}Y |
|
| 715.3026 | 1.5 |
|
Annotations: ^{0,4}A_{GalNAc}Y |
|
| 716.2728 | 1.5 |
|
Annotations: ^{1,3}X_{NeuAc} |
|
| 716.3339 | 1.0 |
|
Annotations: ^{1,3}X_{NeuAc} |
|
| 716.7711 | 1.1 |
| 729.2518 | 1.9 |
|
Annotations: ^{3,5}A_{GalNAc}Y |
|
| 729.2702 | 1.2 |
|
Annotations: ^{3,5}A_{GalNAc}Y |
|
| 729.7537 | 2.5 |
| 733.2868 | 18.7 |
|
Annotations: YY |
|
| 734.2853 | 2.5 |
| 734.3143 | 1.7 |
| 738.2586 | 42.8 |
|
Annotations: |
|
| 738.7569 | 31.2 |
| 739.2701 | 7.2 |
| 749.2574 | 1.9 |
| 752.2714 | 2.2 |
| 757.2768 | 1.6 |
|
Annotations: B^{1,3}X_{NeuAc} |
|
| 759.3235 | 1.1 |
|
Annotations: C^{1,3}X_{Fuc} |
|
| 770.3244 | 1.0 |
| 775.2969 | 1.2 |
|
Annotations: C^{1,3}X_{NeuAc} |
|
| 790.2177 | 1.2 |
| 794.2928 | 3.4 |
| 795.2273 | 1.2 |
| 795.2804 | 1.1 |
| 798.3062 | 1.4 |
| 801.2799 | 3.1 |
|
Annotations: ^{2,5}X_{NeuAc}Z |
|
| 803.2969 | 1.0 |
|
Annotations: ^{0,2}X_{NeuAc}Y |
|
| 812.2753 | 1.7 |
| 813.2774 | 1.2 |
| 813.3059 | 1.6 |
| 819.2816 | 3.6 |
|
Annotations: C |
|
| 820.2867 | 4.3 |
| 820.3207 | 1.3 |
| 835.2878 | 1.3 |
| 842.3092 | 37.3 |
|
Annotations: ZZ |
|
| 843.3001 | 5.3 |
| 843.3329 | 2.2 |
| 843.3617 | 1.7 |
| 844.3178 | 6.2 |
| 860.3174 | 5.0 |
|
Annotations: YZ |
|
| 861.2957 | 4.3 |
|
Annotations: ^{0,4}A_{GalNAc} |
|
| 861.3191 | 1.8 |
|
Annotations: ^{0,4}A_{GalNAc} |
|
| 891.3249 | 5.3 |
|
Annotations: ^{0,3}A_{GalNAc} |
|
| 892.3249 | 3.2 |
| 895.3017 | 1.4 |
|
Annotations: YY |
|
| 895.3308 | 12.8 |
|
Annotations: YY |
|
| 895.3698 | 4.8 |
|
Annotations: YY |
|
| 896.333 | 5.9 |
| 896.3734 | 3.0 |
| 897.3449 | 4.8 |
| 947.3451 | 1.6 |
|
Annotations: ^{0,2}X_{NeuAc}Z |
|
| 949.4421 | 1.2 |
|
Annotations: ^{1,5}X_{NeuAc}Z |
|
| 962.3815 | 1.0 |
|
Annotations: ^{0,4}X_{Fuc}Z |
|
| 963.3269 | 1.0 |
|
Annotations: ^{2,5}X_{NeuAc}Z |
|
| 963.3951 | 1.0 |
|
Annotations: ^{2,5}X_{NeuAc}Z |
|
| 965.3463 | 9.3 |
|
Annotations: Y^{0,2}X_{NeuAc} |
|
| 965.3795 | 3.0 |
|
Annotations: Y^{0,2}X_{NeuAc} |
|
| 966.3492 | 8.5 |
|
Annotations: ^{3,5}X_{Fuc}Y |
|
| 967.3732 | 4.2 |
|
Annotations: ^{1,5}X_{NeuAc}Y |
|
| 981.3297 | 2.6 |
|
Annotations: ^{2,5}X_{NeuAc}Y |
|
| 981.3794 | 1.0 |
|
Annotations: ^{2,5}X_{NeuAc}Y |
|
| 988.3533 | 7.1 |
| 989.3661 | 1.4 |
| 1006.3768 | 11.5 |
|
Annotations: Z |
|
| 1007.3784 | 15.4 |
| 1008.3695 | 2.9 |
| 1022.3441 | 1.0 |
|
Annotations: YZ |
|
| 1022.3873 | 2.4 |
|
Annotations: YZ |
|
| 1024.387 | 10.6 |
|
Annotations: Y |
|
| 1025.3606 | 2.2 |
| 1025.4187 | 2.9 |
| 1040.3721 | 5.2 |
|
Annotations: YY |
|
| 1040.4039 | 1.5 |
|
Annotations: YY |
|
| 1041.3732 | 3.2 |
| 1042.3987 | 1.5 |
| 1127.394 | 1.6 |
| 1143.4396 | 1.8 |
| 1168.4123 | 7.2 |
|
Annotations: Z |
|
| 1168.4451 | 5.5 |
|
Annotations: Z |
|
| 1168.4936 | 1.7 |
|
Annotations: Z |
|
| 1168.9467 | 1.0 |
| 1169.3994 | 1.8 |
| 1169.4342 | 4.2 |
| 1169.4825 | 1.3 |
| 1170.4375 | 1.2 |
| 1186.0973 | 1.7 |
| 1186.4318 | 100.0 |
|
Annotations: Y |
|
| 1186.5477 | 1.5 |
|
Annotations: Y |
|
| 1186.5794 | 1.3 |
|
Annotations: Y |
|
| 1186.9384 | 1.3 |
| 1187.2068 | 1.5 |
| 1187.3149 | 1.3 |
| 1187.4389 | 71.6 |
| 1187.4992 | 5.6 |
| 1187.5624 | 1.6 |
| 1187.811 | 2.8 |
| 1187.8741 | 1.1 |
| 1187.9757 | 1.1 |
| 1188.1221 | 1.3 |
| 1188.1892 | 2.5 |
| 1188.2349 | 1.0 |
| 1188.3568 | 1.0 |
| 1188.435 | 25.3 |
| 1188.527 | 1.6 |
| 1189.2036 | 1.5 |
| 1189.3751 | 1.0 |
| 1189.4351 | 7.3 |
| 1189.8097 | 1.3 |
| 1283.8725 | 1.0 |