Structure

    redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6b1D-GlcNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd

Effects of size and geographical origin on Atlantic salmon, Salmo salar, mucin O-glycan repertoire

PubMed Entry

GlyTouCan Accession Number: Loading...

Peak Intensity
406.12 0.4
407.09 0.9

Annotations:

YZ redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
407.85 0.5
424.3 1.7

Annotations:

^{0,4}A_{GalNAc}Y a1D-GalNAc,p/#acleavage_0_4--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
434.18 0.5
501.3 0.3
510.09 2.0

Annotations:

B ?1HexNAc,p/#bcleavage--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
527.17 1.8

Annotations:

^{2,4}X_{Gal}Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#xcleavage_2_4)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd ^{0,4}X_{GalNAc} redEnd--??1D-GalNAc,p--3a1D-GalNAc,p/#xcleavage_0_4--3?1D-Gal,p$MONO,Und,-H,0,redEnd
527.92 1.0

Annotations:

C ?1HexNAc,p/#ccleavage--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
548.97 0.9

Annotations:

BZ ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd BZ a1D-GalNAc,p/#bcleavage--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd
567.06 0.7

Annotations:

BY ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd CZ ?1D-GalNAc,p/#ccleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd BY a1D-GalNAc,p/#bcleavage--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd CZ a1D-GalNAc,p/#ccleavage--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd
567.96 0.5
569.15 1.3

Annotations:

Z redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd
570.24 2.7
587.3 5.1

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
609.16 1.2

Annotations:

^{0,4}A_{GalNAc}Z a1D-GalNAc,p/#acleavage_0_4--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p/#zcleavage$MONO,Und,-H,0,redEnd
629.51 0.4
665.23 0.5
683.14 0.4
688.1 0.5
689.21 0.4
712.11 4.2

Annotations:

^{2,4}X_{GalNAc}Z redEnd--??1D-GalNAc,p--3a1D-GalNAc,p/#xcleavage_2_4--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd
712.35 3.7
713.06 5.0

Annotations:

B a1D-GalNAc,p/#bcleavage--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
713.36 3.2
713.99 0.6
724.04 0.8
729.43 0.5
730.14 11.8

Annotations:

^{2,4}X_{GalNAc}Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p/#xcleavage_2_4--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
731.18 0.8

Annotations:

C a1D-GalNAc,p/#ccleavage--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
731.47 0.8
748.24 1.1
749.38 0.9
755.03 0.3
772.25 4.8

Annotations:

Z redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
773.18 100.3

Annotations:

^{0,4}A_{GalNAc} a1D-GalNAc,p/#acleavage_0_4--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
774.37 1.0
790.35 5.0

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd YY redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
791.38 1.1
802.45 0.5
810.26 0.4
833.31 0.3
874.17 0.5
874.97 0.6
875.25 1.2
880.7 0.6
886.3 0.5
892.21 5.5
892.57 1.1
894.3 0.4
905.16 0.5
910.19 0.7
910.48 0.7
916.38 0.8

Annotations:

BY ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd CZ ?1D-GalNAc,p/#ccleavage--3a1D-GalNAc,p(--3?1D-Gal,p/#zcleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
917.15 0.4
918.35 1.6
936.19 0.5
945.26 0.7
952.38 4.6

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
953.46 1.0
993.14 0.5

Annotations:

YY redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd
1017.2 1.0
1018.57 0.5
1029.13 0.5
1029.81 0.7
1031.46 0.5
1036.23 0.5
1047.51 1.1
1059.47 0.3
1077.08 1.5
1078.48 1.0

Annotations:

B ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
1079.16 8.0

Annotations:

^{2,4}X_{GalNAc} redEnd--??1D-GalNAc,p--3a1D-GalNAc,p/#xcleavage_2_4--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
1079.43 3.0
1089.42 0.8
1097.1 0.7
1097.51 0.9
1098.17 0.4
1109.29 0.5
1118.89 0.3
1119.35 0.6
1139.09 2.0

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
1139.52 1.7
1139.74 0.5

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p/#ycleavage)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p$MONO,Und,-H,0,redEnd
1140.46 1.3
1151.25 2.3
1154.98 0.6

Annotations:

Y redEnd--??1D-GalNAc,p--3a1D-GalNAc,p(--3?1D-Gal,p)--6?1HexNAc,p--??1D-Gal,p--??1HexNAc,p--??1L-Fuc,p/#ycleavage$MONO,Und,-H,0,redEnd
1181.31 1.3
1187.46 0.4
1193.55 2.8
1199.41 3.2
1217.61 0.6
1223.13 0.6
1241.33 142.2
1242.36 11.7
1242.75 2.3
1259.33 21.2
1260.4 2.5
1260.67 0.9
1265.6 0.6
1302.37 27.6

There are 6 similar spectra:

Id Structure Score

1.00

5761

0.82

4822

0.59

0.59

5471

0.52

5472

0.50

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 1300.51
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Salmo Salar
Tissue - Mucus

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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