Structure

    redEnd--??1D-GalNAc,p(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd

Sulfation of O-glycans on mucin-type proteins from serous ovarian epithelial tumors

GlyTouCan Accession Number: Loading...

Peak Intensity
240.79 0.1

Annotations:

B ?1D-GalNAc,p/#bcleavage--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
241.11 1.5

Annotations:

B ?1D-GalNAc,p/#bcleavage--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
242.07 0.2
257.99 0.4

Annotations:

^{3,5}A_{GalNAc}Z ?1D-GalNAc,p/#acleavage_3_5--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
259.13 0.5

Annotations:

C ?1D-GalNAc,p/#ccleavage--3b1D-Gal,p--6?1S$MONO,Und,-H,0,redEnd
259.69 0.0
362.78 0.2
388.94 0.2

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
407.03 0.7

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
407.24 0.2

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
408.3 0.1
422.66 0.1
429.05 0.2
446.29 0.3

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p/#zcleavage$MONO,Und,-H,0,redEnd
464.19 6.4

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p/#ycleavage$MONO,Und,-H,0,redEnd
464.78 0.0
465.29 0.5
473.23 0.3
505.14 0.3
527.33 0.2
538.81 0.6

Annotations:

^{1,5}A_{GalNAc}Y ?1D-GalNAc,p/#acleavage_1_5(--3b1D-Gal,p--6?1S/#lcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
539.36 0.0

Annotations:

^{1,5}A_{GalNAc}Y ?1D-GalNAc,p/#acleavage_1_5(--3b1D-Gal,p--6?1S/#lcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
547.1 0.4
548.09 0.4

Annotations:

^{2,5}A_{GalNAc}Y ?1D-GalNAc,p/#acleavage_2_5(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
548.63 0.0
558.97 0.3
576.92 0.8
577.47 0.0
588.16 0.6
588.7 0.0
589.14 0.5
589.69 0.0
595.17 0.3
598.52 1.1
599.06 0.0
606.33 0.6
607.16 0.6
607.72 0.0
613.27 0.5
613.82 0.0
616.86 0.6
635.17 0.2
649.14 1.0

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p--4b1D-Gal,p/#zcleavage$MONO,Und,-H,0,redEnd
650.06 0.2
650.59 0.1
651.19 0.4
652.09 0.7
652.65 0.0
667.19 42.4

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p--4b1D-Gal,p/#ycleavage$MONO,Und,-H,0,redEnd
668.17 7.7
669.0 0.0
670.86 0.3
680.39 1.1
680.95 0.0
686.96 0.5
687.52 0.0
691.08 0.2
695.15 0.8
695.7 0.0
701.71 0.3

Annotations:

^{1,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_1_5(--3b1D-Gal,p--6?1S/#lcleavage)--6b1D-GlcNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
710.33 0.6

Annotations:

^{2,5}A_{GalNAc} ?1D-GalNAc,p/#acleavage_2_5(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
710.87 0.0
711.45 0.6
712.01 0.0
729.08 0.1
737.74 0.7
738.29 0.0
740.74 0.3
755.07 0.3
758.12 0.4
760.74 0.4
761.29 0.0
763.96 0.3
766.92 0.2
767.73 0.2
768.55 0.5
769.12 2.3
769.69 0.0
770.07 0.4
770.48 0.9
771.04 0.0
782.66 0.4
784.24 0.9
784.63 1.2
784.92 1.2
785.48 0.0
786.06 0.6
786.62 0.0
787.08 0.5
787.26 0.6
787.8 0.0
788.36 1.0
788.93 0.0
793.51 0.5
799.33 0.2
803.9 0.6
804.45 0.0
828.91 0.5

Annotations:

redEnd--??1D-GalNAc,p(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
829.34 0.8

Annotations:

redEnd--??1D-GalNAc,p(--3b1D-Gal,p--6?1S)--6b1D-GlcNAc,p--4b1D-Gal,p$MONO,Und,-H,0,redEnd
830.18 0.4

There are 20 similar spectra:

Id Structure Score

1.00

6689

0.99

0.99

5568

0.98

3122

0.97

3499

0.96

5392

0.96

0.96

6651

0.96

0.96

0.95

3123

0.92

0.91

0.90

6652

0.89

0.89

6686

0.88

0.88

5783

0.86

6727

0.81

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 828.25
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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