Structure

    redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd

Rainbow trout gastrointestinal mucus, mucin production, mucin glycosylation and response to lipopolysaccharide

GlyTouCan Accession Number: Loading...

Peak Intensity
194.24 3.1
210.14 2.5
272.14 4.1

Annotations:

BZ ?1D-GalNAc,p/#bcleavage--6a2D-NeuAc,p--8a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
289.3 2.8
290.12 832.7

Annotations:

B a2D-NeuAc,p/#bcleavage--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd B b1D-Gal,p/#bcleavage--3a2D-NeuAc,p$MONO,Und,-H,0,redEnd
291.17 86.9
292.03 3.2
299.2 3.0

Annotations:

C ?1D-GalNAc,p/#ccleavage--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd
380.26 17.0
381.47 2.9
385.24 2.9
398.25 3.2
407.76 3.3
414.27 3.0
429.31 11.5
443.85 15.0
444.38 6.9
460.03 2.6
461.3 3.2
464.35 3.8
471.41 2.5
473.8 17.9

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p/#zcleavage$MONO,Und,-2H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#zcleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd
478.35 13.1
482.79 199.9

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-2H,0,redEnd Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-2H,0,redEnd
483.29 106.7
483.81 4.5
493.33 4.3
501.43 3.4
504.86 5.2
507.07 4.7
510.13 2.8
511.37 5.7

Annotations:

^{0,2}A_{NeuAc} a2D-NeuAc,p/#acleavage_0_2--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
513.1 3.9

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
519.52 11.9
520.28 5.0
522.87 5.9
537.32 133.9
538.03 6.7
538.39 18.4
541.44 4.2
547.08 17.2
549.74 3.0
554.24 2.8
559.36 3.8
563.23 3.4
565.38 4.4
566.13 24.0
567.16 8.4
567.44 3.4
567.85 3.7
568.12 2.8
571.96 5.9
574.1 2.7
575.5 3.4
580.29 7.5
581.27 1217.0

Annotations:

B ?1D-GalNAc,p/#bcleavage--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
582.28 234.7
583.23 11.6
583.58 8.3
584.08 11.3
584.52 6.2
584.82 3.9
585.21 8.5
585.89 4.4
592.44 6.7
592.88 3.8
593.25 7.6
597.35 22.0
597.99 17.6
598.38 6.9
598.71 3.4
599.37 3.5

Annotations:

C ?1D-GalNAc,p/#ccleavage--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
655.38 3.4
656.34 5.4
657.29 19.1

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#zcleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
673.25 11.0
673.49 5.9
675.37 2341.4

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
676.49 320.4
677.49 26.0
708.12 6.0
742.47 2.9
806.62 3.5
888.75 3.6
904.37 2.7
922.37 25.5
922.79 5.9
923.51 13.7
930.61 4.9
931.49 2.7
932.38 5.5
946.81 2.7
948.51 41.8

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#zcleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
948.99 3.3
949.56 17.4
964.46 6.1
965.27 11.7
966.42 730.0

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p)--6a2D-NeuAc,p--8a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--3a2D-NeuAc,p/#ycleavage)--6a2D-NeuAc,p--8a2D-NeuAc,p$MONO,Und,-H,0,redEnd
967.41 289.3
968.53 15.5

There are not related spectra

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 1256.44
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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