Structure

    redEnd--??1D-GalNAc,p(--??1D-Gal,p)--??2D-NeuAc,p--??1S$MONO,Und,-H,0,redEnd

The O-glycome of human nigrostriatal tissue and its alteration in Parkinsons disease

GlyTouCan Accession Number: Loading...

Peak Intensity
239.54 0.3
240.99 5.3
249.28 0.4
251.02 0.8
256.19 0.3
258.59 0.4
260.8 0.4
290.04 0.7

Annotations:

B ?1D-GalNAc,p/#bcleavage--??2D-NeuAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
290.26 0.6

Annotations:

B ?1D-GalNAc,p/#bcleavage--??2D-NeuAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
295.33 0.4
308.3 0.6

Annotations:

C ?1D-GalNAc,p/#ccleavage--??2D-NeuAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
326.17 1.3
350.29 0.3
368.12 0.4
370.15 11.7

Annotations:

B ?1D-GalNAc,p/#bcleavage--??2D-NeuAc,p--??1S$MONO,Und,-H,0,redEnd
371.98 0.3
376.02 0.3
383.36 0.4
399.26 0.4
416.3 0.3
424.3 0.3
440.65 0.3
444.18 0.4
457.05 0.5
458.02 0.3
461.26 0.3
462.29 0.9
463.29 0.4
464.2 687.4
465.18 0.8
466.24 0.9
468.11 0.3
474.11 0.3
482.35 0.3
487.48 0.3
488.11 0.4
490.55 0.3
496.4 0.4
497.29 0.3
515.27 0.5
523.09 0.3
526.15 0.4
532.27 0.6
534.53 0.6
539.29 0.3
540.81 0.3
542.33 0.4
543.05 0.4
546.31 0.8
547.4 0.4
551.17 0.3
563.56 0.7
565.09 0.5
567.41 0.3
597.44 1.0
599.75 0.5
601.34 0.4
609.32 0.4
610.34 0.7
612.16 0.3
613.49 0.5
614.21 0.4
615.1 0.3
619.21 0.3
620.44 1.2
622.54 0.3
629.37 0.4
633.41 0.4
637.59 0.4
638.4 0.7
639.04 0.3
639.38 0.4
640.29 0.4
649.25 0.3
656.4 0.3
657.4 2.2
659.3 0.4
667.99 0.5
671.39 0.3
672.63 0.4
673.42 0.6
674.45 0.5
675.35 108.0

Annotations:

redEnd--??1D-GalNAc,p(--??1D-Gal,p)--??2D-NeuAc,p--??1S/#lcleavage$MONO,Und,-H,0,redEnd
679.75 0.6
680.46 0.4
694.6 0.5
695.3 4.5
696.12 0.8
696.65 0.3
697.81 0.3
709.26 0.6
711.34 62.4
712.18 0.7
715.36 0.8
719.36 0.4
727.33 0.8
727.61 0.4
728.03 0.5
729.41 0.3
736.41 0.4

There are 14 similar spectra:

Id Structure Score

5714

1.00

6586

1.00

5429

1.00

4850

1.00

3497

1.00

7626

0.99

5713

0.99

7183

0.99

7695

0.99

7434

0.99

7405

0.99

7170

0.99

7690

0.98

7683

0.98

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 754.21
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Homo Sapiens
Tissue - Brain

HPLC

Column

Method

  • 78 min gradient with approx 3-5 ul/min (static split from 250 ul/min) run rate
  • 10 mM (NH4)HCO3
  • 10 mM (NH4)HCO3 in 80% acetonitrile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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