Structure

    redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd

Rainbow trout gastrointestinal mucus, mucin production, mucin glycosylation and response to lipopolysaccharide

GlyTouCan Accession Number: Loading...

Peak Intensity
348.17 1.7

Annotations:

B b1D-Gal,p/#bcleavage--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
348.71 0.0
407.39 1.0

Annotations:

YZ redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p/#ycleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p/#zcleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
458.96 0.5
479.25 2.0
479.86 0.0
484.99 0.7
527.36 4.4
527.59 2.3
528.18 0.0

Annotations:

C a1D-GalNAc,p/#ccleavage--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p$MONO,Und,-H,0,redEnd
551.27 0.6

Annotations:

ZZ redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
569.2 3.0

Annotations:

YZ redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
569.79 0.0
570.31 0.3
587.33 20.3

Annotations:

YY redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
588.03 0.0
588.51 0.3
597.36 0.7
607.3 1.3
607.86 0.0
622.42 4.8
622.98 0.0
657.17 1.9
657.71 0.0
675.63 1.0
682.06 0.6
682.43 1.2
682.97 0.0
692.72 0.4
717.62 2.1
718.19 0.0
724.26 1.6
724.8 0.0
725.56 1.0
726.11 0.0
800.19 7.5
800.59 1.0
801.35 0.5
816.25 1.5
816.79 0.0
818.38 1.0
842.19 2.0
842.73 0.0
859.5 1.7
860.05 0.0
860.45 1.7

Annotations:

Z redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
860.67 1.2
861.21 0.0
878.06 0.6
878.57 4.8

Annotations:

Y redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
879.16 0.0
885.15 0.6
900.33 2.6
900.89 0.0
918.31 2.7

Annotations:

Z redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
918.52 2.1
918.88 1.0
919.44 0.0
934.29 2.2
934.86 0.0
936.05 1.2
936.59 5.6

Annotations:

Y redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
937.57 1.6
938.12 0.0
985.48 1.7
986.03 0.0
988.18 1.1
988.59 1.4
989.14 0.0
1006.1 2.0
1006.58 13.5

Annotations:

^{0,2}X_{NeuAc} redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p)--6a2D-NeuAc,p/#xcleavage_0_2$MONO,Und,-H,0,redEnd
1006.9 1.5
1007.39 0.5
1024.68 1.6
1025.23 0.0
1029.58 1.8
1030.16 0.0
1045.69 2.9
1046.27 0.0
1059.59 0.7
1066.67 2.5
1067.22 0.0
1074.44 1.6
1075.02 0.0
1076.87 0.4
1081.47 0.6

Annotations:

Y redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p--3b1D-Gal,p--??1D-GalNAc,p--3a1L-Fuc,p/#ycleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
1101.71 1.9
1102.27 0.0
1149.54 2.8
1149.81 4.9
1150.32 1.5
1150.87 0.0
1166.81 2.8
1167.61 42.5
1168.02 8.5
1168.46 5.9
1168.81 0.3
1185.47 0.8
1191.41 4.7
1191.96 0.0

There are 7 similar spectra:

Id Structure Score

4899

0.89

0.89

4900

0.88

0.88

5464

0.88

7186

0.78

5835

0.75

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 1226.47
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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