Structure

    redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd

Gill mucus and gill mucin O-glycosylation in healthy and amebic gill disease affected Atlantic salmon

GlyTouCan Accession Number: Loading...

Peak Intensity
274.39 1.4

Annotations:

Z^{0,2}X_{NeuAc} redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6a2D-NeuAc,p/#xcleavage_0_2$MONO,Und,-H,0,redEnd
278.18 1.1
290.13 73.3

Annotations:

B ?1D-GalNAc,p/#bcleavage--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
291.26 5.4
308.2 2.9

Annotations:

C ?1D-GalNAc,p/#ccleavage--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
316.43 1.1
318.06 0.9
324.22 1.5
346.0 0.8
364.0 3.3

Annotations:

B ?1D-GalNAc,p/#bcleavage--3b1D-Gal,p--??1HexNAc,p$MONO,Und,-H,0,redEnd
364.26 1.0
366.1 1.7

Annotations:

YZ redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p/#ycleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p/#zcleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
384.08 2.8

Annotations:

YY redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p/#ycleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
384.35 1.0
407.35 0.8
411.07 2.4
412.98 1.2
417.07 1.1
435.2 1.8
435.41 1.1
447.25 0.7
451.38 1.3
453.12 2.0

Annotations:

^{2,4}X_{GalNAc} redEnd--??1D-GalNAc,p/#xcleavage_2_4--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
455.11 1.0
459.19 1.3
472.38 1.2
474.84 1.2
477.28 6.7
479.22 1.3
493.16 0.7
495.25 0.8

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#zcleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
513.25 3.6

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p/#ycleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
513.97 4.5
543.34 0.7
553.29 0.8
567.54 1.6
568.73 1.0
569.44 5.7

Annotations:

Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
570.15 3.0
583.07 0.8
587.26 76.5

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
588.2 12.4
588.53 3.8
597.56 1.8
615.28 4.7
616.1 3.2
621.29 0.9
628.98 1.4
629.43 1.5
630.21 1.4
632.44 0.8
638.52 0.8
639.02 1.5
639.38 6.0
650.43 1.2
655.97 2.2
656.18 1.0
657.26 38.1

Annotations:

^{0,2}X_{NeuAc} redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p)--6a2D-NeuAc,p/#xcleavage_0_2$MONO,Und,-H,0,redEnd Z redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p/#zcleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
657.97 2.7
658.23 2.9
658.64 1.0
675.21 20.5

Annotations:

Y redEnd--??1D-GalNAc,p(--3b1D-Gal,p--??1HexNAc,p/#ycleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
676.41 5.5
676.69 1.4
680.56 2.2
710.13 1.6
712.2 1.2
734.84 1.5
740.21 2.1
740.47 2.3
742.03 0.8
749.41 1.0
758.37 0.7
770.04 1.6
770.3 0.9
771.43 1.3
776.97 2.9
778.35 4.5
779.1 5.0
780.05 1.5
780.37 4.2
799.31 0.7
800.28 22.0
800.76 1.8
801.29 8.3
809.69 0.9
817.04 1.4
818.31 161.1
819.33 22.2
820.99 2.7
828.27 3.7
836.26 2.2
836.9 1.5
837.53 1.0
841.49 1.4
842.75 6.4
843.35 2.2
850.52 0.7
879.42 3.2
880.93 2.0

There are 20 similar spectra:

Id Structure Score

6806

0.96

4858

0.96

0.96

7148

0.95

5721

0.88

5722

0.86

4808

0.84

0.84

8001

0.82

5785

0.82

5436

0.81

7409

0.81

7438

0.81

7149

0.78

5520

0.70

5570

0.59

6805

0.54

6807

0.52

7218

0.51

6734

0.51

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 877.33
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

Taxonomy - Salmo Salar
Tissue - Gills

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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