Structure

    redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd

Rainbow trout gastrointestinal mucus, mucin production, mucin glycosylation and response to lipopolysaccharide

GlyTouCan Accession Number: Loading...

Peak Intensity
202.14 4.3

Annotations:

B ?1D-GalNAc,p/#bcleavage--3a1D-GalNAc,p$MONO,Und,-H,0,redEnd
204.05 22.4

Annotations:

YZ redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd ZY redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
208.04 3.8
210.14 4.5
212.04 1.6
220.03 10.1

Annotations:

C ?1D-GalNAc,p/#ccleavage--3a1D-GalNAc,p$MONO,Und,-H,0,redEnd
229.83 2.9
246.02 2.5
272.13 30.0
275.95 4.3
276.38 1.8
282.18 3.6
286.79 2.2
289.13 1.6
290.13 1833.7

Annotations:

B ?1D-GalNAc,p/#bcleavage--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
291.31 2.3
308.14 76.8

Annotations:

C ?1D-GalNAc,p/#ccleavage--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
310.25 1.6
321.08 2.8
347.4 2.4
365.2 14.0
367.97 2.0
387.31 2.6
389.18 2.3
391.06 6.2
391.34 2.4
405.16 22.3
405.39 7.6
407.23 92.8

Annotations:

Z redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p)--6a2D-NeuAc,p/#zcleavage$MONO,Und,-H,0,redEnd
412.33 2.2
417.16 4.2
417.59 2.0
421.3 1.6
425.3 298.0

Annotations:

Y redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p)--6a2D-NeuAc,p/#ycleavage$MONO,Und,-H,0,redEnd
426.67 2.6
429.14 16.9
429.44 6.2
431.18 2.9
433.4 7.4
435.11 6.3
441.15 3.3
447.11 3.6
448.06 2.3
451.28 21.1
451.51 15.2
459.73 3.0
467.31 17.6
477.28 93.0
494.33 1.6
495.17 38.2

Annotations:

Z redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p/#zcleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd ^{0,2}X_{NeuAc} redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p)--6a2D-NeuAc,p/#xcleavage_0_2$MONO,Und,-H,0,redEnd
495.44 24.3
495.9 1.5
496.38 1.8
497.29 2.2
513.18 2.6

Annotations:

Y redEnd--??1D-GalNAc,p(--3a1D-GalNAc,p/#ycleavage)--6a2D-NeuAc,p$MONO,Und,-H,0,redEnd
513.48 2.0
514.11 9.8
514.58 2.1
515.14 4.3
515.39 5.1
518.17 7.0
518.51 5.5
520.29 2.5
523.37 1.6
530.68 3.7
542.33 2.3
548.0 3.8
548.49 9.3
552.31 1.9
555.16 3.2
571.3 2.7
578.43 4.1
593.13 1.8
593.92 2.9
594.22 3.8
594.56 2.1
608.32 4.6
612.05 2.3
612.46 4.0
615.45 2.2
622.48 2.4
624.19 1.5
638.46 77.6
646.7 1.7
654.45 5.4
655.47 3.8
656.35 375.2
656.98 3.7
670.93 1.5
672.21 5.0
672.47 6.6
673.66 1.8
674.19 1.7
679.15 2.2
680.49 41.8
685.04 3.1
685.58 4.0
686.34 2.4
689.48 3.1
755.21 3.5

There are 26 similar spectra:

Id Structure Score

6713

1.00

5424

1.00

5773

1.00

5705

1.00

4803

0.99

0.99

7182

0.99

7393

0.99

7422

0.99

7144

0.99

7988

0.98

5772

0.98

5553

0.98

5704

0.97

4845

0.97

0.97

3750

0.97

0.97

0.97

7166

0.96

6712

0.96

7987

0.96

0.95

0.95

5512

0.95

5513

0.90

Structure Format

SNFG Oxford Text

Structure details

Reducing Mass: 715.28
(Calculated Monoisotopic)

Reducing End: Reduced

Persubstitution: Underivatised

Biological Context

N/A

HPLC

Column

Method

  • 40 min gradient with 10 ul/min run rate
  • 10 mM (NH4)HCO3 in water
  • 10 mM (NH4)HCO3 in 80% acetontirile

Mass Spec

Thermo Fisher LTQ Linear Ion Trap ESI

MIRAGE Structural data

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